Pharmacopoeial Analysis 2 - Practice

Daten

Offizielle Daten in der Fachveröffentlichung für das folgende akademische Jahr: 2024-2025

Thematik

Within the frame of the theoretical and practical trainings of this subject students will study the quantitative approach of chemical analysis. This approach is crucial for the study of almost all fields of the pharmaceutical sciences such as pharmaceutical chemistry, pharmaceutical technology etc. Students have to learn and examine the theory and practice of the quantitative analytical reactions, methods, rules and calculations.

Vorlesungen

Praktika

• 1. Laboratory safety and accident protection. Calibration of glassware.
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  2. Laboratory safety and accident protection. Calibration of glassware.
• 3. Laboratory safety and accident protection. Calibration of glassware.
• 4. Calibration of glassware.
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  5. Calibration of glassware.
• 6. Calibration of glassware.
• 7. Standardization of 0.1 M hydrochloric acid solution.
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  8. Standardization of 0.1 M hydrochloric acid solution.
• 9. Standardization of 0.1 M hydrochloric acid solution.
• 10. Standardization of 0.1 M sodium hydroxide measuring solution.
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  11. Standardization of 0.1 M sodium hydroxide measuring solution.
• 12. Standardization of 0.1 M sodium hydroxide measuring solution.
• 13. Parallel determination of boric acid and borax (sodium tetraborate) by alkalimetry and acidimetry.
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  14. Parallel determination of boric acid and borax (sodium tetraborate) by alkalimetry and acidimetry.
• 15. Parallel determination of boric acid and borax (sodium tetraborate) by alkalimetry and acidimetry.
• 16. Parallel determination of sodium hydroxide and sodium carbonate by Warder's method.
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  17. Parallel determination of sodium hydroxide and sodium carbonate by Warder's method.
• 18. Parallel determination of sodium hydroxide and sodium carbonate by Warder's method.
• 19. Parallel determination of sodium hydrogen carbonate and sodium carbonate by Warder's method.
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  20. Parallel determination of sodium hydrogen carbonate and sodium carbonate by Warder's method.
• 21. Parallel determination of sodium hydrogen carbonate and sodium carbonate by Warder's method.
• 22. Determination of acetic acid. Determination of acetate ions under non-aqueous conditions.
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  23. Determination of acetic acid. Determination of acetate ions under non-aqueous conditions.
• 24. Determination of acetic acid. Determination of acetate ions under non-aqueous conditions.
• 25. Parallel complexometric determination of calcium and magnesium ions.
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  26. Parallel complexometric determination of calcium and magnesium ions.
• 27. Parallel complexometric determination of calcium and magnesium ions.
• 28. Complexometric determination of nickel (II) ions. Determination of aluminum ions by indirect titration.
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  29. Complexometric determination of nickel (II) ions. Determination of aluminum ions by indirect titration.
• 30. Complexometric determination of nickel (II) ions. Determination of aluminum ions by indirect titration.
• 31. Standardization of 0.02 M potassium permanganate solution.
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  32. Standardization of 0.02 M potassium permanganate solution.
• 33. Standardization of 0.02 M potassium permanganate solution.
• 34. Permanganometric determination of hydrogen peroxide. Permanganometric determination of iron (II) ions.
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  35. Permanganometric determination of hydrogen peroxide. Permanganometric determination of iron (II) ions.
• 36. Permanganometric determination of hydrogen peroxide. Permanganometric determination of iron (II) ions.
• 37. Standardization of 0.01 M sodium thiosulfate measuring solution. Determination of copper (II) ions.
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  38. Standardization of 0.01 M sodium thiosulfate measuring solution. Determination of copper (II) ions.
• 39. Standardization of 0.01 M sodium thiosulfate measuring solution. Determination of copper (II) ions.
• 40. Determination of chloride ions by Mohr's method.
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  41. Determination of chloride ions by Mohr's method.
• 42. Determination of chloride ions by Mohr's method.

Seminare

Materialien zum Aneignen des Lehrstoffes

Obligatorische Literatur

Harris D.C.: Quantitative Chemical Analysis, 8th ed., W.H. Freeman and Co., New York, 2010.

Vom Institut veröffentlichter Lehrstoff

Laboratory handouts - describing details of the experiments.

Skript

Empfohlene Literatur

Voraussetzung zum Absolvieren des Semesters

Acknowledgement of the course is in accord with the Code of Studies and Examinations. Participation in the practices of the course is obligatory. Maximum 3 absences are allowed.

Semesteranforderungen

At least 75% of the quantitative determinations should be at least satisfactory. Students write at least four mini-tests on the practices. The average of their results must be at least 50%. The practical work (results of the written tests and the experimental work) is evaluated by a practical grade. Satisfactory (2) evaluation is the minimum requirement of acknowledgment of the semester.

Möglichkeiten zur Nachholung der Fehlzeiten

There is no opportunity to make up missed classes (lectures and practices).

Prüfungsfragen

N/A

Prüfer

Praktika, Seminarleiter/innen

• Kulcsár Győző Kornél
• Tyukodi Levente