Pharmacopoeial Analysis 2. - practice

Daten

Offizielle Daten in der Fachveröffentlichung für das folgende akademische Jahr: 2019-2020

Thematik

Within the frame of the theoretical and practical trainings of this subject students will study the quantitative approach of chemical analysis. This approach is crucial for the study of almost all fields of the pharmaceutical sciences such as pharmaceutical chemistry, pharmaceutical technology etc. Students have to learn and examine the theory and practice of the quantitative analytical reactions, methods, rules and calculations.

Vorlesungen

Praktika

• 1. Acceptance of lab equipment, stock-taking, fire prevention and safety education. General introduction. Measurements. Calibration.
• 2. Acceptance of lab equipment, stock-taking, fire prevention and safety education. General introduction. Measurements. Calibration.
• 3. Acceptance of lab equipment, stock-taking, fire prevention and safety education. General introduction. Measurements. Calibration.
• 4. General introduction. Measurements. Calibration.
• 5. General introduction. Measurements. Calibration.
• 6. General introduction. Measurements. Calibration.
• 7. Factor for 0.1 M hydrochloric acid solution.
• 8. Factor for 0.1 M hydrochloric acid solution.
• 9. Factor for 0.1 M hydrochloric acid solution.
• 10. Factor for 0.1 M sodium hydroxide solution.
• 11. Factor for 0.1 M sodium hydroxide solution.
• 12. Factor for 0.1 M sodium hydroxide solution.
• 13. Acid-base titrations I. Titration of acetic acid using sodium hydroxide. Determination of potassium acetate in glacial acetic acid medium.
• 14. Acid-base titrations I. Titration of acetic acid using sodium hydroxide. Determination of potassium acetate in glacial acetic acid medium.
• 15. Acid-base titrations I. Titration of acetic acid using sodium hydroxide. Determination of potassium acetate in glacial acetic acid medium.
• 16. Acid-base titrations II. Determination of borax (sodium tetraborate) by alkalimetry and acidimetry.
• 17. Acid-base titrations II. Determination of borax (sodium tetraborate) by alkalimetry and acidimetry.
• 18. Acid-base titrations II. Determination of borax (sodium tetraborate) by alkalimetry and acidimetry.
• 19. Acid-base titrations III. Indirect determination of thiosulfate by alkalimetry. Parallel determination of sodium carbonate and sodium hydrogencarbonate by Warder's method.
• 20. Acid-base titrations III. Indirect determination of thiosulfate by alkalimetry. Parallel determination of sodium carbonate and sodium hydrogencarbonate by Warder's method.
• 21. Acid-base titrations III. Indirect determination of thiosulfate by alkalimetry. Parallel determination of sodium carbonate and sodium hydrogencarbonate by Warder's method.
• 22. Complexometry I.: Determination of calcium and magnesium ion sin the presence of each other.
• 23. Complexometry I.: Determination of calcium and magnesium ion sin the presence of each other.
• 24. Complexometry I.: Determination of calcium and magnesium ion sin the presence of each other.
• 25. Complexometry II.: Determination of nickel (II) ions. Determination of aluminium ions by reverse titration.
• 26. Complexometry II.: Determination of nickel (II) ions. Determination of aluminium ions by reverse titration.
• 27. Complexometry II.: Determination of nickel (II) ions. Determination of aluminium ions by reverse titration.
• 28. Redox titrations I. - Permanganometry. Factor for 0.02 M potassium permanganate measuring solution. Determination of calcium ions by reverse titration.
• 29. Redox titrations I. - Permanganometry. Factor for 0.02 M potassium permanganate measuring solution. Determination of iron(II) by permanganate titration.
• 30. Redox titrations I. - Permanganometry. Factor for 0.02 M potassium permanganate measuring solution. Determination of calcium ions by reverse titration.
• 31. Redox titrations II. - Permanganometry. Determination of hydrogen peroxide. Determination of iron (II) ions.
• 32. Redox titrations II. - Permanganometry. Determination of hydrogen peroxide. Determination of iron (II) ions.
• 33. Redox titrations II. - Permanganometry. Determination of hydrogen peroxide. Determination of iron (II) ions.
• 34. Redox titrations III. - Iodometry. Factor for 0.01 M sodium thiosulfate measuring solution. Determination of copper (II) ions.
• 35. Redox titrations III. - Iodometry. Factor for 0.01 M sodium thiosulfate measuring solution. Determination of copper (II) ions.
• 36. Redox titrations III. - Iodometry. Factor for 0.01 M sodium thiosulfate measuring solution. Determination of copper (II) ions.
• 37. Redox titrations IV. - Iodometry. Determination of hydrogen peroxide. Determination of water by Karl-Fischer method.
• 38. Redox titrations IV. - Iodometry. Determination of hydrogen peroxide. Determination of water by Karl-Fischer method.
• 39. Redox titrations IV. - Iodometry. Determination of hydrogen peroxide. Determination of water by Karl-Fischer method.
• 40. Precipitate formation titrations. - Argentometry. Determination of chloride ions by Volhard's method and by Mohr's method.
• 41. Precipitate formation titrations. - Argentometry. Determination of chloride ions by Volhard's method and by Mohr's method.
• 42. Precipitate formation titrations. - Argentometry. Determination of chloride ions by Volhard's method and by Mohr's method.

Seminare

Materialien zum Aneignen des Lehrstoffes

Obligatorische Literatur

Harris D.C.: Quantitative Chemical Analysis, 8th ed., W.H. Freeman and Co., New York, 2010.

Vom Institut veröffentlichter Lehrstoff

Laboratory handouts - describing details of the experiments.

Skript

Empfohlene Literatur

Voraussetzung zum Absolvieren des Semesters

Acknowledgement of the course is in accord with the Code of Studies and Examinations. Participation in the practices of the course is obligatory. Maximum 3 absences are allowed. Students have to write at least four mini-tests on the practices. The average of the results must be at least 50%. The practical work (results of the written tests and the experimental work) is evaluated by a practical grade. Satisfactory (2) evaluation is the minimum requirement of acknowledgement of the semester.

Semesteranforderungen

Möglichkeiten zur Nachholung der Fehlzeiten

There is no opportunity to make up missed classes (lectures and practices).

Prüfungsfragen

Prüfer

Praktika, Seminarleiter/innen

• Dr. Almási Attila
• Dr. Kulcsár Győző Kornél