Daten
Offizielle Daten in der Fachveröffentlichung für das folgende akademische Jahr: 2020-2021
Lehrbeauftragte/r
-
Dr. Cecilia PÁPAY- SÁR
associate professor,
Department of Organic and Pharmacological Chemistry -
Semesterwochenstunden
Vorlesungen: 0
Praktika: 0
Seminare: 24
Insgesamt: 24
Fachangaben
- Kode des Kurses: OPE-SME-T
- 2 kredit
- Pharmacy
- Elective modul
- spring
OPA-S1E-T completed
Zahl der Kursteilnehmer für den Kurs:
min. 2 – max. 10
Thematik
The aim of this course is to introduce the students how to identify organic compounds from the complementary information afforded by three types of spectra: infrared, mass and NMR.
Vorlesungen
Praktika
Seminare
- 1. Infrared Spectroscopy: Introduction, theory, instrumentation, interpretation of spectra
- 2. Infrared Spectroscopy: Introduction, theory, instrumentation, interpretation of spectra
- 3. Infrared Spectroscopy: Characteristic group absorptions of organic molecules
- 4. Infrared Spectroscopy: Characteristic group absorptions of organic molecules
- 5. Infrared Spectroscopy: Solving problems
- 6. Infrared Spectroscopy: Solving problems
- 7. Proton Magnetic Resonance Spectrometry (1H NMR): Introduction, theory, instrumentation
- 8. Proton Magnetic Resonance Spectrometry (1H NMR): Introduction, theory, instrumentation
- 9. 1H NMR: Chemical shift, simple spin coupling
- 10. 1H NMR: Chemical shift, simple spin coupling
- 11. 1H NMR: Protons on heteroatoms, chemical shift equivalence and magnetic equivalence, effects of a chiral center
- 12. 1H NMR: Protons on heteroatoms, chemical shift equivalence and magnetic equivalence, effects of a chiral center
- 13. 13 C NMR Spectroscopy: Interpretation of 13 C spectra. The principles of MRI
- 14. 1H NMR and 13 C NMR: Solving problems
- 15. Mass Spectrometry: Mass spectrometer parts, ionization processes
- 16. Mass Spectrometry: Mass spectrometer parts, ionization processes
- 17. Mass Spectrometry: Appearance of the mass spectrum, mass spectra of classes of organic compounds
- 18. Mass Spectrometry: Appearance of the mass spectrum, mass spectra of classes of organic compounds
- 19. Mass Spectrometry: Interpretation of the mass spectrum through examples
- 20. Mass Spectrometry: Interpretation of the mass spectrum through examples
- 21. Summary of spectroscopic methods: identification of organic molecules from IR, NMR and mass spectra
- 22. Summary of spectroscopic methods: identification of organic molecules from IR, NMR and mass spectra
- 23. Summary of spectroscopic methods: identification of organic molecules from IR, NMR and mass spectra
- 24. Evaluation, written test
Materialien zum Aneignen des Lehrstoffes
Obligatorische Literatur
Silverstein, R.M., Webster, F.X., Kiemle, D.: Spectrometric Identification of Organic Compounds, John Wiley and Sons, 2005.
Vom Institut veröffentlichter Lehrstoff
The ppt slides are uploaded to Neptun Meet Street.
Skript
Empfohlene Literatur
Voraussetzung zum Absolvieren des Semesters
Maximum of 25 % absence allowed
Semesteranforderungen
The student who has been absent from more than 25 % of the classes cannot be granted to entry of exam.
Möglichkeiten zur Nachholung der Fehlzeiten
Students can personally consult with the lecturer.
Prüfungsfragen
Infrared Spectroscopy: theory, instrumentation, interpretation of spectra, chacteristic group absorptions of organic molecules.
Proton Magnetic Resonance Spectrometry (1H NMR): theory, instrumentation, chemical shift, simple spin coupling, protons on heteroatoms, chemical shift equivalence and magnetic equivalence, effects of a chiral center.
Mass Spectrometry: mass spectrometer parts, ionization processes, appearance of the mass spectrum, mass spectra of classes of organic compounds.
Identification of simple organic molecules from IR, NMR and mass spectra.
Prüfer
Praktika, Seminarleiter/innen
- Dr. Kálai Tamás
- Pápayné Dr. Sár Cecilia