Adatok
A Tantárgybejelentőben megadott hivatalos adatok az alábbi tanévre: 2020-2021
Tantárgyfelelős
-
Dr. Cecilia PÁPAY- SÁR
associate professor,
Department of Organic and Pharmacological Chemistry
Óraszámok/félév
előadás: 0 óra
gyakorlat: 0 óra
szeminárium: 24 óra
összesen: 24 óra
Tárgyadatok
- Kód: OPE-SME-T
- 2 kredit
- Pharmacy
- Elective modul
- spring
OPA-S1E-T completed
Kurzus létszámkorlát
min. 2 fő – max. 10 fő
Tematika
The aim of this course is to introduce the students how to identify organic compounds from the complementary information afforded by three types of spectra: infrared, mass and NMR.
Előadások
Gyakorlatok
Szemináriumok
- 1. Infrared Spectroscopy: Introduction, theory, instrumentation, interpretation of spectra
- 2. Infrared Spectroscopy: Introduction, theory, instrumentation, interpretation of spectra
- 3. Infrared Spectroscopy: Characteristic group absorptions of organic molecules
- 4. Infrared Spectroscopy: Characteristic group absorptions of organic molecules
- 5. Infrared Spectroscopy: Solving problems
- 6. Infrared Spectroscopy: Solving problems
- 7. Proton Magnetic Resonance Spectrometry (1H NMR): Introduction, theory, instrumentation
- 8. Proton Magnetic Resonance Spectrometry (1H NMR): Introduction, theory, instrumentation
- 9. 1H NMR: Chemical shift, simple spin coupling
- 10. 1H NMR: Chemical shift, simple spin coupling
- 11. 1H NMR: Protons on heteroatoms, chemical shift equivalence and magnetic equivalence, effects of a chiral center
- 12. 1H NMR: Protons on heteroatoms, chemical shift equivalence and magnetic equivalence, effects of a chiral center
- 13. 13 C NMR Spectroscopy: Interpretation of 13 C spectra. The principles of MRI
- 14. 1H NMR and 13 C NMR: Solving problems
- 15. Mass Spectrometry: Mass spectrometer parts, ionization processes
- 16. Mass Spectrometry: Mass spectrometer parts, ionization processes
- 17. Mass Spectrometry: Appearance of the mass spectrum, mass spectra of classes of organic compounds
- 18. Mass Spectrometry: Appearance of the mass spectrum, mass spectra of classes of organic compounds
- 19. Mass Spectrometry: Interpretation of the mass spectrum through examples
- 20. Mass Spectrometry: Interpretation of the mass spectrum through examples
- 21. Summary of spectroscopic methods: identification of organic molecules from IR, NMR and mass spectra
- 22. Summary of spectroscopic methods: identification of organic molecules from IR, NMR and mass spectra
- 23. Summary of spectroscopic methods: identification of organic molecules from IR, NMR and mass spectra
- 24. Evaluation, written test
A tananyag elsajátításához szükséges segédanyagok
Kötelező irodalom
Silverstein, R.M., Webster, F.X., Kiemle, D.: Spectrometric Identification of Organic Compounds, John Wiley and Sons, 2005.
Saját oktatási anyag
The ppt slides are uploaded to Neptun Meet Street.
Jegyzet
Ajánlott irodalom
A félév elfogadásának feltételei
Maximum of 25 % absence allowed
Félévközi ellenőrzések
The student who has been absent from more than 25 % of the classes cannot be granted to entry of exam.
Távolmaradás pótlásának lehetőségei
Students can personally consult with the lecturer.
Vizsgakérdések
Infrared Spectroscopy: theory, instrumentation, interpretation of spectra, chacteristic group absorptions of organic molecules.
Proton Magnetic Resonance Spectrometry (1H NMR): theory, instrumentation, chemical shift, simple spin coupling, protons on heteroatoms, chemical shift equivalence and magnetic equivalence, effects of a chiral center.
Mass Spectrometry: mass spectrometer parts, ionization processes, appearance of the mass spectrum, mass spectra of classes of organic compounds.
Identification of simple organic molecules from IR, NMR and mass spectra.
Vizsgáztatók
Gyakorlatok, szemináriumok oktatói
- Dr. Kálai Tamás
- Pápayné Dr. Sár Cecilia